HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Cymene → 5,5-dimethyl-10-hydroxy-8-methyl-5H-[1]benzopyrano[3,4-d]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Cymene | HCID 7463 | — |
| Reactant | 2-benzyl-10-hydroxy-5,5,8-trimethyl-1,2,3,4-tetrahydro-5H[1]benzopyrano[3,4-d]pyridine | HCID 21532612 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 5,5-dimethyl-10-hydroxy-8-methyl-5H-[1]benzopyrano[3,4-d]pyridine | HCID 20287837 | — |
Reaction Steps
Reaction of 2-benzyl-10-hydroxy-5,5,8-trimethyl-1,2,3,4-tetrahydro-5H[1]benzopyrano[3,4-d]pyridine (100 mg., U.S. Pat. No. 3,535,327) with Pd/C in boiling cymene gives 10-hydroxy-5,5,8-trimethyl-5H[1]benzopyrano[3,4-d]pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962448 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-30da125517fe4424b733ceeeeeb4de79 |
| Source note | uspto-grants-1976_06 |