Nitric Acid → HCID 54732702, compound

Participants

Reaction Conditions

Reaction Steps

To a stirred suspension of 1,6-dimethyl-4-hydroxy carbostyril (1.70g; 0.009 mole) in glacial acetic acid (10 ml) was added concentrated nitric acid (2.5 ml; d, 1.42) with swirling. The solid dissolved on warming to 100°C to give a red solution which precipitated the 3-nitro compound as yellow crystals on cooling. m.p. 185°C. (Found: C, 56.05; H, 4.33; N, 11.86%, C11H10N2O4 requires; C, 56.41; H, 4.30; N, 11.96%).

Provenance & Evidence