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HRID 1658111作成日:2026年10月25日

3-Phenoxy-alpha-ethynylbenzylalcohol → 2,2-Dimethylspiro[2,4]heptane-1-carboxylic acid, alpha-ethynyl-m-phenoxybenzyl ester

https://huagongshe.com/reaction/1658111

反応式

関与物質

役割名称HCID仕込み量
反応物3-Phenoxy-alpha-ethynylbenzylalcoholHCID 12919092—
反応物HCID 20531773HCID 20531773—
生成物2,2-Dimethylspiro[2,4]heptane-1-carboxylic acid, alpha-ethynyl-m-phenoxybenzyl esterHCID 86733552—

反応手順

The procedure of Example 1 is followed using 2,2-dimethylspiro[2,4]heptane-1-carboxylic acid in place of 2,2-dimethyl-4,5-benzospiro[2,4]hepta-4,6-diene-1-carboxylic acid and α-ethynyl-m-phenoxybenzyl alcohol in place of m-phenoxybenzyl alcohol to give the product as an oil.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US03962458
出典データセットuspto-grants-1976_06
ORD IDord-c6168f0715ac49eea7c9c10ae4bd0cbc
出典メモuspto-grants-1976_06