HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Pentylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Pentylbenzoic acid | HCID 33479 | — |
| Product | 4-Pentylbenzoyl chloride | HCID 170812 | — |
Reaction Steps
15 g. of p-n-pentylbenzoic acid are dissolved in 100 ml. of thionyl chloride and boiled at reflux for 1 hour. The excess thionyl chloride is then removed by distillation and the acid chloride is distilled under high vacuum. The p-n-pentylbenzoic acid chloride which is obtained has a boiling point of 104°C/2 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963313 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-46ae8f63b7a944168dc866d8c849d353 |
| Source note | uspto-grants-1976_06 |