Aniline → HCID 21528839, compound

HRID 1658201Notes

Reaction equation

HRID 1658201 reaction equation
Cl[CH2:2][C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:8][C:7]=1[Cl:16])=[O:4].[NH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:18]1([NH:17][CH2:2][C:3]([NH:5][C:6]2[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:8][C:7]=2[Cl:16])=[O:4])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 215288302-chloro-N-(2-chloro-4-sulfamoylphenyl)acetamide

Product 1

HCID 21528839HCID 21528839, compound

Procedure

2-Chloro-N-(2-chloro-4-sulphamoylphenyl)-acetamide (28.3g 0.1 mole) and aniline (18.6g, 0.2 mole) were heated together for 30 min. on a water bath (90°). The mixture was worked up as in Example 1(b) to yield 20.8 g m.p. 185°-186°

Workup

  1. customto yield 20.8 g m.p. 185°-186°

Sources & evidence

ORD record
ord-ea17e947341c49b696770eb8f5de896d
Source dataset
uspto-grants-1976_06
Patent number
US03963706

Reaction notes

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