Aniline → HCID 21528845, compound

HRID 1658204Notes

Reaction equation

HRID 1658204 reaction equation
Cl[CH2:2][C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[C:8]([Cl:16])[CH:7]=1)=[O:4].[NH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:18]1([NH:17][CH2:2][C:3]([NH:5][C:6]2[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[C:8]([Cl:16])[CH:7]=2)=[O:4])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 21528855HCID 21528855, compound

Product 1

HCID 21528845HCID 21528845, compound

Procedure

2-Chloro-N-(3-chloro-4-sulphamoylphenyl)-acetamide (28.3 g) and aniline (19 ml) were heated together for 30 min on a water bath (90°) and the product worked up as in Example 1(b) to yield 25 g, m.p. 192°-194°.

Workup

  1. customto yield 25 g, m.p. 192°-194°

Sources & evidence

ORD record
ord-3e3225e41ee24ab4ab7035994f8e872d
Source dataset
uspto-grants-1976_06
Patent number
US03963706

Reaction notes

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