HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → Benzenesulfonamide, 2-chloro-4-(5-oxo-3-phenyl-1-imidazolidinyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 21528845 | HCID 21528845 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | Benzenesulfonamide, 2-chloro-4-(5-oxo-3-phenyl-1-imidazolidinyl)- | HCID 3041005 | — |
Reaction Steps
2-Phenylamino-N-(3-chloro-4-sulphamoylphenyl)-acetamide (34 g) was dissolved in ethanol (300 ml) and paraformaldehyde (6.0 g) in water (600 ml) added. The mixture was refluxed 4 hrs and cooled. The product was worked up as in Example 1(c) to yield: 18 g, m.p. 257°-259°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-08a3c4f3aa924cee884ea89ee6375cab |
| Source note | uspto-grants-1976_06 |