HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → 2-Chloro-N-(2-methyl-4-sulphamoylphenyl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | 4-Amino-3-methylbenzene-1-sulfonamide | HCID 143037 | — |
| Product | 2-Chloro-N-(2-methyl-4-sulphamoylphenyl)-acetamide | HCID 21528849 | — |
Reaction Steps
2-methyl-4-sulphamoylaniline (18,6 g) and α-chloroacetyl chloride (30g) were refluxed together 30 min. and the mixture worked up as in Example 2(a) to yield 11 g, m.p. 193°-194°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-af1623bdbf9c4a9ea3f1a88efd2e675b |
| Source note | uspto-grants-1976_06 |