HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-Phenylamino-N-(2-methyl-4-sulphamoylphenyl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Chloro-N-(2-methyl-4-sulphamoylphenyl)-acetamide | HCID 21528849 | — |
| Product | 2-Phenylamino-N-(2-methyl-4-sulphamoylphenyl)-acetamide | HCID 21528856 | 44% |
Reaction Steps
2-Chloro-N-(2-methyl-4-sulphamoylphenyl)-acetamide (13.1g) and aniline (9.5 g) were heated together 21/2 hr on a water bath at 90°. The mixture was worked up as in Example 1(b) to yield 7 g beige crystals, m.p. 195°-196°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-a25644f5dae245b39611f5eb2fbb0219 |
| Source note | uspto-grants-1976_06 |