4-Chloroaniline → HCID 21528863, compound

HRID 1658215Notes

Reaction equation

HRID 1658215 reaction equation
Cl[CH2:2][C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:8][C:7]=1[Cl:16])=[O:4].[Cl:17][C:18]1[CH:24]=[CH:23][C:21]([NH2:22])=[CH:20][CH:19]=1>>[Cl:17][C:18]1[CH:24]=[CH:23][C:21]([NH:22][CH2:2][C:3]([NH:5][C:6]2[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:8][C:7]=2[Cl:16])=[O:4])=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 78124-ChloroanilineHCID 215288302-chloro-N-(2-chloro-4-sulfamoylphenyl)acetamide

Product 1

HCID 21528863HCID 21528863, compound

Procedure

2-Chloro-N-(2-chloro-4-sulphamoylphenyl)-acetamide (7g) and p-chloroaniline (6.3 g) were heated together for 45 minutes on a water bath at 90°. The mixture was worked up as in Example 1(b) to yield the title product (4.5 g), m.p. 185° .

Sources & evidence

ORD record
ord-649d00de258c40b7af887d705844aa6e
Source dataset
uspto-grants-1976_06
Patent number
US03963706

Reaction notes

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