HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → Acetanilide, 2-chloro-4'-nitro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | 4-Nitroaniline | HCID 7475 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Acetanilide, 2-chloro-4'-nitro- | HCID 140220 | — |
Reaction Steps
p-Nitroaniline (10.0g) and chloroacetyl chloride (15 ml) were refluxed together 1 hour, mixed with ethyl acetate and washed with water 3 times to yield 11.5 g; mp 183°-185°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-e971da8fca1a4d0b865e66110d0e7741 |
| Source note | uspto-grants-1976_06 |