Ethanol → HCID 21528862, compound

HRID 1658222Notes

Reaction equation

HRID 1658222 reaction equation
[CH:1]1([NH:7][CH2:8][C:9]([NH:11][C:12]2[CH:17]=[CH:16][C:15]([N+:18]([O-:20])=[O:19])=[CH:14][CH:13]=2)=[O:10])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH2:21](O)C>O>[CH:1]1([N:7]2[CH2:8][C:9](=[O:10])[N:11]([C:12]3[CH:13]=[CH:14][C:15]([N+:18]([O-:20])=[O:19])=[CH:16][CH:17]=3)[CH2:21]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 702EthanolHCID 2990118HCID 2990118, compound

Product 1

HCID 21528862HCID 21528862, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

2-Cyclohexylamino-N-(4-nitrophenyl)-acetamide (3.5g) were added to ethanol (85 ml). p-Formaldehyde (0.8g) in water (110 ml) was added and the mixture was refluxed 4 hours, cooled and filtered to yield 3.1 g, m.p. 132°-133°C

Workup

  1. temperaturethe mixture was refluxed 4 hours
  2. temperaturecooled
  3. filtrationfiltered
  4. customto yield 3.1 g, m.p. 132°-133°C

Sources & evidence

ORD record
ord-c4c29ea664214e3cbd161b3e8f146870
Source dataset
uspto-grants-1976_06
Patent number
US03963706

Reaction notes

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