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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1658224Generated: November 2, 2026

m-Toluidine → HCID 21528850, compound

https://huagongshe.com/reaction/1658224

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-ToluidineHCID 7934—
Reactant2-chloro-N-(2-chloro-4-sulfamoylphenyl)acetamideHCID 21528830—
SolventEthanolHCID 702—
ProductHCID 21528850HCID 2152885063.3%

Reaction Steps

2-Chloro-N-(2-chloro-4-sulphamoylphenyl)-acetamide (28.3 g) and m-toluidine (31.8 g) were heated 7 hours at 175°C (oil bath) and worked up as in Example 15 to yield 22.4 g product, m.p. 185°-189°C (ethanol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03963706
Source datasetuspto-grants-1976_06
ORD IDord-accb0fb798104155af3dd0d0b868d4d8
Source noteuspto-grants-1976_06