HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfanilamide → HCID 21528871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfanilamide | HCID 5333 | — |
| Reactant | Chloroacetanilide | HCID 11485 | — |
| Product | HCID 21528871 | HCID 21528871 | — |
Reaction Steps
α-Chloracetanilide (17.0 g) and sulfanilamide (34.5 g) were heated together in an autoclave for 8 hours at 120°C. The mixture was triturated with 2N HCl and filtered to yield 27.5 g, m.p. 257°-258°C (acetone).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-7d724319f7d4407e80a7cd4d58458005 |
| Source note | uspto-grants-1976_06 |