HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 12720209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 5,5,7,7-tetramethyl-4-oxido-3-phenylfuro[3,4-e][1,2,4]triazin-4-ium | HCID 6412720 | — |
| Product | HCID 12720209 | HCID 12720209 | — |
Reaction Steps
A mixture of 5.42 g. (0.02 mole) 5,7-dihydro-5,5,7,7-tetramethyl-3-phenylfuro[3,4-e]-as-triazine-4-oxide and 70 ml. triethylphosphite is refluxed under nitrogen for 18 hours at a bath temperature of 180°C. The solvent is removed in vacuo and the residue recrystallized from aqueous ethanol to give 5,7-dihydro-5,5,7,7-tetramethyl-3-phenylfuro[3,4-e]-as-triazine, m.p. 90°-91°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963713 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-effd520d555e4ae5b65d2b63b182c8d4 |
| Source note | uspto-grants-1976_06 |