Bromine → HCID 21529338, compound

HRID 1658385Notes

Reaction equation

HRID 1658385 reaction equation
[C:1]([C:4]1[CH:5]=[C:6]([CH:10]([CH3:16])[C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:7]=[CH:8][CH:9]=1)(=[O:3])[CH3:2].[Cl-].[Al+3].[Cl-].[Cl-].[Br:21]Br>CCOCC>[Br:21][CH2:2][C:1]([C:4]1[CH:5]=[C:6]([CH:10]([CH3:16])[C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:7]=[CH:8][CH:9]=1)=[O:3]

Participants

5

Reactant 3

HCID 24408BromineHCID 6451240Aluminum(III) ChlorideHCID 12356932HCID 12356932, compound

Product 1

HCID 21529338HCID 21529338, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To a cooled vigorously stirred mixture containing ethyl 2-(m-acetyl phenyl)propionate (0.1 mole) dissolved in dry ether (100 ml) and a pinchful of aluminum chloride is added dropwise 0.1 mole bromine.

Workup

  1. temperatureTo a cooled vigorously stirred mixture

Sources & evidence

ORD record
ord-0b38972e4a144aa2ab82083bd55fc310
Source dataset
uspto-grants-1976_06
Patent number
US03963758

Reaction notes

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