N-(2-Octyl)-p-phenylenediamine → N-(3-isopropoxypropyl)-N'-(2-octyl)-p-phenylenediamine

HRID 1658450Notes

Reaction equation

HRID 1658450 reaction equation
[CH3:1][CH:2]([NH:9][C:10]1[CH:15]=[CH:14][C:13]([NH2:16])=[CH:12][CH:11]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH:17]([O:20][CH2:21][CH2:22][CH2:23]Br)([CH3:19])[CH3:18]>C1(N)C(F)=C(F)C(F)=C(N)C=1F.Cl.Cl>[CH:17]([O:20][CH2:21][CH2:22][CH2:23][NH:16][C:13]1[CH:14]=[CH:15][C:10]([NH:9][CH:2]([CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH3:1])=[CH:11][CH:12]=1)([CH3:19])[CH3:18]

Participants

4

Reactant 2

HCID 584493N-(2-Octyl)-p-phenylenediamineHCID 126137771-Bromo-3-(propan-2-yloxy)propane

Product 1

HCID 21529417N-(3-isopropoxypropyl)-N'-(2-octyl)-p-phenylenediamine

Reagents, catalysts & solvents 1

HCID 149026Tetrafluoro-m-phenylenediamine dihydrochlorideSolvent

Procedure

Following the same conditions as in Example 4, but reacting N-(2-octyl)-p-phenylenediamine with 3-isopropoxypropyl bromide, there is obtained the title product in dihydrochloride salt form (m.p. 200°-202°C).

Sources & evidence

ORD record
ord-fc76a3d3f5db4b978435754771643334
Source dataset
uspto-grants-1976_06
Patent number
US03963780

Reaction notes

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