HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanate → HCID 53841590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Reactant | 1,12-Dodecanediamine | HCID 17727 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 53841590 | HCID 53841590 | — |
Reaction Steps
22 grams (.110 mole) of 1,12-diaminododecane in 300 cc ether was reacted via dropwise addition with 5 grams (0.058 mole) ethyl isothiocyanate. The precipitate was filtered, washed with ether and recrystallized from alcohol yielding 6 grams of the thiourea derivative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965015 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-b9b9cbaea4fb49c5b11de92462b2e838 |
| Source note | uspto-grants-1976_06 |