Hexamethylenediamine → HCID 53642786, compound

HRID 1658471Notes

Reaction equation

[CH2:1]([NH2:8])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH2:7].[CH2:9]([N:27]=[C:28]=[O:29])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[CH2:9]([NH:27][C:28]([NH:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][NH2:8])=[O:29])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

Reactant 2

HCID 16402Hexamethylenediamine

HCID 66988Octadecyl isocyanate

Product 1

HCID 53642786HCID 53642786, compound

Procedure

29 grams 1,6-hexanediamine (0.25 mole) was reacted with 20 gms (0.068 mole) octadecyl isocyanate as in Example 2. Yield: 25.5 gms, melting point 123°-168°C.

Sources & evidence

ORD record: ord-485ec3885fee4f3a9fd3c35b8e8fd524
Source dataset: uspto-grants-1976_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03965015

Reaction notes

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