1,8-Octanediamine → HCID 54521374, compound

HRID 1658472Notes

Reaction equation

HRID 1658472 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][NH2:10].[CH2:11]([N:29]=[C:30]=[O:31])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]>>[CH2:11]([NH:29][C:30]([NH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][NH2:10])=[O:31])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]

Participants

3

Reactant 2

HCID 242501,8-OctanediamineHCID 66988Octadecyl isocyanate

Product 1

HCID 54521374HCID 54521374, compound

Procedure

36 grams (.25 mole) of 1,8 diaminooctane was reacted with 20 gms (0.068 mole) octadecyl isocyanate as in Example 2. Yield: 26.6 gms, melting point 120°-145°-156°C.

Workup

  1. customYield: 26.6 gms, melting point 120°-145°-156°C.

Sources & evidence

ORD record
ord-9b75a4c17bc04478b9b202d3b07b99c8
Source dataset
uspto-grants-1976_06
Patent number
US03965015

Reaction notes

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