HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediamine → HCID 53801695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediamine | HCID 428 | — |
| Reactant | Butyl isocyanate | HCID 8110 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 53801695 | HCID 53801695 | — |
Reaction Steps
30 grams 1,3 diaminopropane in 30 mls ether was slowly (1 hour) reacted with 10 gms butyl isocyanate and refluxed for one-half hour. The precipitate was filtered and washed with ether and dried in vacuum oven, melting point 201°-202°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965015 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-354a92a97dbb4d83a40a89bca30fb9f9 |
| Source note | uspto-grants-1976_06 |