Benzyl Bromide → HCID 12354099, compound

Participants

Reaction Steps

A stirred mixture of 6.1 g. of 2,3-dihydro-5-hydroxycyclopenta[d]pyrido[1,2-a]pyrimidin-10(1H)-one, 1.40 g. of powdered sodium hydroxide, 100 ml of xylene, 100 mg of copper bronze, and 6.2 g. of benzyl bromide are stirred and heated under reflux for 12 hours, and filtered hot. From the filtrate, on cooling, the product crystallizes. It is filtered and recrystallized from xylene to give 6.3 g. of product, m.p. 150°-152°.

Provenance & Evidence