HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86733570, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2,4-Dimethyl-4-nitrodecahydropyrido[1,2-a][1,4]diazepine | HCID 12339509 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86733570 | HCID 86733570 | — |
Reaction Steps
Under agitation, a solution of 2.27 g. of 2,4-dimethyl-4-nitroperhydropyrido[1,2-a] [1,4] diazepine in 10 ml. of ethyl acetate is added to 20 ml. of 2N ethereal hydrochloric acid. The residue remaining after concentration is crystallized from chloroform; m.p. 189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965103 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-b2b1d4974385403ea4406162fc457004 |
| Source note | uspto-grants-1976_06 |