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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1658553Generated: November 3, 2026

Methanol → Methyl 7-methyl-9H-xanthene-2-carboxylate

https://huagongshe.com/reaction/1658553

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSulfuric AcidHCID 1118—
Reactant7-Methyl-9H-xanthene-2-carboxylic acidHCID 21500671—
SolventWaterHCID 962—
ProductMethyl 7-methyl-9H-xanthene-2-carboxylateHCID 21500836—

Reaction Conditions

Temperature40 °C

Reaction Steps

Twenty-six grams of 7-methylxanthene-2-carboxylic acid is added to 400 ml. of absolute methanol. To the resultant solution are added 18 ml. of concentrated sulfuric acid and the mixture is then heated at reflux for about two hours. The mixture is then cooled to 40°C and sufficient water is added to bring the total volume to 1400 ml. The resultant mixture is then filtered to give methyl 7-methylxanthene-2-carboxylate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03965115
Source datasetuspto-grants-1976_06
ORD IDord-ec23fa05a1c048889a3a63d776f77737
Source noteuspto-grants-1976_06