Sodium Hydroxide → HCID 53964741, compound

HRID 1658557Notes

Reaction equation

HRID 1658557 reaction equation
Cl.[CH3:2][N:3]([CH3:13])[CH:4]=[C:5]([C:11]#[N:12])[CH:6]=[N:7][N:8]([CH3:10])[CH3:9].[OH-].[Na+]>O>[CH3:13][N:3]([CH3:2])[CH:4]=[C:5]([C:11]#[N:12])[CH:6]=[N:7][N:8]([CH3:10])[CH3:9]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 86733582HCID 86733582, compound

Product 1

HCID 53964741HCID 53964741, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Of the N-(3-dimethylamino-2-cyano-2-propene-1-ylidene)-N',N'-dimethylhydrazine hydrochloride was dissolved in the minimum required amount of water. The pH was adjusted to 8 by addition of 10% sodium hydroxide solution. The desired product N-(3-dimethylamino-2-cyano-2-propene-1-ylidene)-N',N'-dimethylhydrazine precipitated and was filtered off (m.p. 130°-134°).

Workup

  1. customThe desired product N-(3-dimethylamino-2-cyano-2-propene-1-ylidene)-N',N'-dimethylhydrazine precipitated
  2. filtrationwas filtered off (m.p. 130°-134°)

Sources & evidence

ORD record
ord-7181a783437646aea23f7a6d01c79e32
Source dataset
uspto-grants-1976_06
Patent number
US03965141

Reaction notes

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