HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenethylamine → 5-chloro-2-methoxy-N-(2-phenylethyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenethylamine | HCID 1001 | — |
| Edukt | 5-Chlorosalicylic Acid | HCID 9447 | — |
| Edukt | 5-chloro-2-methoxy-N-(2-(4-sulfamoylphenyl)ethyl)benzamide | HCID 85542 | — |
| Edukt | Methyl 5-chloro-2-methoxybenzoate | HCID 118574 | — |
| Produkt | 5-chloro-2-methoxy-N-(2-phenylethyl)benzamide | HCID 118575 | — |
Reaktionsschritte
A process for preparing p-(2-{5-chloro-2-methoxybenzamido}ethyl)-benzene sulfonamide which comprises the steps of methylating 5-chlorosalicylic acid to methyl-5-chloro-2-methoxybenzoate, treating methyl-5-chloro-2-methoxybenzoate with phenethylamine to obtain N-phenethyl-5-chloro-2-methoxybenzamide, subjecting said N-phenethyl-5-chloro-2-methoxybenzamide to chlorosulfonation and aminolysis to yield p-(2-{5-chloro-2-methoxybenzamido}ethyl)-benzene sulfonamide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03965173 |
| Quelldatensatz | uspto-grants-1976_06 |
| ORD ID | ord-93d9fbeb860f44d2955f8e87a3177b3f |
| Quellennotiz | uspto-grants-1976_06 |