HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → Diphenyl chlorophosphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Phosphorodichloridic acid, phenyl ester | HCID 13038 | — |
| Product | Diphenyl chlorophosphate | HCID 75654 | — |
Reaction Steps
To the reaction mixture of (1), there is added 188 g. phenol and the temperature is raised to 150°C. for 2 hours. The reaction mixture is alllowed to cool and stripped of phenyl phosphorodichloridate. Distillation of the residue affords principally diphenyl phosphorochloridate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965220 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-ecb9c7c2b33f448e9d66daedf0ddfdfa |
| Source note | uspto-grants-1976_06 |