HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylene Glycol → Isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylene Glycol | HCID 8117 | — |
| Reactant | Toluene 2,4-Diisocyanate | HCID 11443 | — |
| Product | Isocyanate | HCID 105034 | — |
| Product | HCID 86733594 | HCID 86733594 | — |
Reaction Steps
After heating 2 moles of tolylene diisocyanate at 40°C., one mole of diethylene glycol was added dropwise thereto during a period of 3 hours. After completion of the dropping, the reaction was carried out for 2 hours at 60°C. to obtain a diethylene glycol-tolylene diisocyanate adduct of an isocyanate equivalent of 220.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966681 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-f3e2ef5620ad4d18bb584779c94a692b |
| Source note | uspto-grants-1976_06 |