HRID1658697
反应详情
EQUATION
反应方程式
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PRODUCTS
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PROCEDURE
实验过程
N-Benzyloxypyridinium p-toluenesulfonate was prepared by mixing pyridine-N-oxide and an equimolar amount of benzyl p-toluenesulfonate and heating the mixture at 85°C for 4 hours. The crude product was recrystallized from a mixture of ethanol and ethyl acetate. By this procedure N-benzyloxypyridinium p-toluenesulfonate having a melting point of 107° to 109°C was obtained.
WORKUP
后处理
- customN-Benzyloxypyridinium p-toluenesulfonate was prepared
- customThe crude product was recrystallized from a mixture of ethanol and ethyl acetate