HRID1658697

反应详情

EQUATION

反应方程式

HRID 1658697 的结构方程式

PROCEDURE

实验过程

N-Benzyloxypyridinium p-toluenesulfonate was prepared by mixing pyridine-N-oxide and an equimolar amount of benzyl p-toluenesulfonate and heating the mixture at 85°C for 4 hours. The crude product was recrystallized from a mixture of ethanol and ethyl acetate. By this procedure N-benzyloxypyridinium p-toluenesulfonate having a melting point of 107° to 109°C was obtained.

WORKUP

后处理

  1. customN-Benzyloxypyridinium p-toluenesulfonate was prepared
  2. customThe crude product was recrystallized from a mixture of ethanol and ethyl acetate