HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrothiophene → HCID 21525294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrothiophene | HCID 1127 | — |
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Product | HCID 21525294 | HCID 21525294 | — |
Reaction Steps
A mixture of 1.76 g of tetrahydrothiophene and 3.72 g of methyl p-toluenesulfonate was allowed to stand for 3 days at room temperature. The crystals which were deposited were collected by filtration, washed with diethyl ether, and dried. By this procedure crystals of S-methyltetrahydrothiophenium p-toluenesulfonate were obtained. After the product was recrystallized, it had a melting point of 145.0° to 148.0°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966720 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-f8fda405e03a4c94afb2ffd6816d8319 |
| Source note | uspto-grants-1976_06 |