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HRID1658775

反应详情

EQUATION

反应方程式

HRID 1658775 的结构方程式

REACTANTS

反应物

2
结构：S=P12SP3(=S)SP(=S)(S1)SP(=S)(S2)S3
HCID14817

Phosphorus pentasulfide

P4S10

结构：O=C1Nc2ccccc2N(C(=O)CN2CCCCC2)c2ncccc21
HCID21525555

未命名化合物

PRODUCTS

生成物

1
结构：O=C(CN1CCCCC1)N1c2ccccc2NC(=S)c2cccnc21
HCID21525538

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

In the manner given in Example 1, 6,11-dihydro-11-(piperidinoacetyl)-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one is reacted with phosphorus pentasulfide in pyridine to give 6,11-dihydro-11-(piperidinoacetyl)-5H-pyrido-[2,3-b][1,5]benzodiazepin-5-thione.