HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 6-Nitroveratrylidenecyclohexylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 6-Nitroveratraldehyde | HCID 88505 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-Nitroveratrylidenecyclohexylamine | HCID 54195554 | 80.4% |
Reaction Steps
A suspension of 42.2 g (0.2 mole) of 6-nitroveratraldehyde, 19.8 g (0.2 mole) cyclohexylamine, 1.0 ml. glacial acetic acid, and 1.25 l. ethanol was stirred and refluxed for five min., cooled, and filtered. The solid was washed with 100 ml. cold ethanol and air dried to give 47.0 g (80%) of the product, m.p. 160°-161°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966760 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-42f980647856479f9946c78ab836389f |
| Source note | uspto-grants-1976_06 |