Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Allyl chloride | HCID 7850 | — |
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Catalyst | Tetraethylammonium Bromide | HCID 6285 | — |
| Product | Methyl sorbate | HCID 5323650 | — |
Reaction Steps
Quantities of 1.9 grams alyl allyl chloride dimer, 2.75 grams tetraethyl ammonium bromide, 5.25 grams of triphenyl phosphine, 45 cc allyl alcohol, and 60 cc methyl acrylate are introduced into a reaction chamber and heated to 120°C for 20 hours. Methyl sorbate is produced to the extent of 10% by weight of the final reaction solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03966798 |
|---|
| Source dataset | uspto-grants-1976_06 |
|---|
| ORD ID | ord-dbee69ccc2334fbdbae0686df9cd869c |
|---|
| Source note | uspto-grants-1976_06 |
|---|
