Phosphorus tribromide → HCID 86733621, compound

HRID 1658920Notes

Reaction equation

HRID 1658920 reaction equation
[CH2:1]([OH:16])[CH2:2][O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][CH2:10][CH2:11][O:12][CH2:13][CH2:14][OH:15].P(Br)(Br)[Br:18]>N1C=CC=CC=1>[Br-:18].[Br-:18].[CH2:14]([OH:15])[CH2:13][O:12][CH2:11][CH2:10][O:9][CH2:8][CH2:7][O:6][CH2:5][CH2:4][O:3][CH2:2][CH2:1][OH:16]

Participants

4

Reactant 2

HCID 24614Phosphorus tribromideHCID 62551Pentaethylene glycol

Product 1

HCID 86733621HCID 86733621, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

In a manner similar to that described in Example 2A, treat pentaethylene glycol with phosphorous tribromide in pyridine. Isolate and purify the resultant product in a manner similar to that described to obtain pentaethylene glycol dibromide.

Workup

  1. customIsolate
  2. custompurify the resultant product in a manner similar to

Sources & evidence

ORD record
ord-16f549a91ffc473e94536f80e86530e5
Source dataset
uspto-grants-1976_06
Patent number
US03966766

Reaction notes

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