2,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzene → HCID 21413090, compound

HRID 1658948Notes

Reaction equation

HRID 1658948 reaction equation
[Cl:1][C:2](=[CH2:5])[CH2:3][NH2:4].[Cl:6][C:7]1[C:12]([N+:13]([O-:15])=[O:14])=[C:11](Cl)[C:10]([N+:17]([O-:19])=[O:18])=[CH:9][C:8]=1[C:20]([F:23])([F:22])[F:21]>C(O)C>[Cl:1][C:2](=[CH2:5])[CH2:3][NH:4][C:11]1[C:10]([N+:17]([O-:19])=[O:18])=[CH:9][C:8]([C:20]([F:21])([F:22])[F:23])=[C:7]([Cl:6])[C:12]=1[N+:13]([O-:15])=[O:14]

Participants

4

Reactant 2

HCID 943982,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzeneHCID 10975406HCID 10975406, compound

Product 1

HCID 21413090HCID 21413090, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The compound was repared by reacting 2-chloroallylamine with 2,4-dichloro-3,5-dinitrobenzotrifluoride in ethanol. After recrystallization from ethanol, the compound melts at 78° - 80°C.

Workup

  1. customAfter recrystallization from ethanol

Sources & evidence

ORD record
ord-9f72a1e719374e1caff1e916ca2bf542
Source dataset
uspto-grants-1976_06
Patent number
US03966816

Reaction notes

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