HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1659067Generated: October 26, 2026
Thionyl Chloride → beta-(2'-Chloro-4-biphenylyl)propionyl chloride
https://huagongshe.com/reaction/1659067
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | beta-(2'-Chloro-4-biphenylyl)propionic acid | HCID 1394276 | — |
| Product | beta-(2'-Chloro-4-biphenylyl)propionyl chloride | HCID 21526230 | — |
Reaction Steps
β-(2'-chloro-4-biphenylyl)propionic acid (26 g.) is treated with thionyl chloride (18 g.) at 0°-5°C. After 10 mins the temperature is raised to 60°C for 30 mins, then the residue is distilled at 0.05 mm to give β-(2'-chloro-4-biphenylyl)propionyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US03966801 |
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| Source dataset | uspto-grants-1976_06 |
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| ORD ID | ord-1cf2ddcaced44d57af0b1b597587984a |
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| Source note | uspto-grants-1976_06 |
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