Diethylamine → HCID 131710373, compound

Participants

Reaction Steps

Anhydrous diethylamine (0.11 moles) is added dropwise to a stirred solution of α-hydroxy-γ-(2'-chloro-4-biphenylyl)butyric acid (0.10 moles) in 100 ml. of n-hexane at 0°C. The precipitated diethylammonium salt is collected on a filter washed with n-hexane and dried in a vacuum desiccator to obtain α-hydroxy-γ-(2'-chloro-4-biphenylyl)butyric acid, diethylammonium salt.

Provenance & Evidence