HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 54246714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 2-(Hydroxyimino)-3-(prop-2-en-1-yl)-1,3-thiazolidin-4-one | HCID 71396854 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 54246714 | HCID 54246714 | — |
Reaction Steps
To a solution of (1.7 g) 3-allyl-2-oximino-4-thiazolidinone in 20 ml of acetone was added 1.0 ml methylisocyanate and 1 drop of triethylamine. The mixture was placed in a pressure bottle and left standing overnight at ambient temperature. The solution was concentrated to a solid residue. Recrystallized from ethyl acetate. Weight 1.7 g. m.p. 108°-110°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966953 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-306d038ac5a64386b367f6d198880f6f |
| Source note | uspto-grants-1976_06 |