Ethanol → HCID 20560004, compound

HRID 1659267Notes

Reaction equation

HRID 1659267 reaction equation
C[C:2]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[N+:16]([O-])=O)=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=1.[CH2:19](O)C>[Pd]>[NH2:16][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=1[CH2:2][CH:3]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=1)[CH3:19]

Participants

4

Reactant 2

HCID 702EthanolHCID 70562833HCID 70562833, compound

Product 1

HCID 20560004HCID 20560004, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

2-(β-Methyl-2-nitrostyryl)pyridine (24.0 g., 0.1 mole) is hydrogenated on a Parr apparatus in 200 ml. of ethanol with 3 g. of 10% Pd/C as catalyst. The catalyst is filtered and the filtrate evaporated, providing 2-[2-(2-aminophenyl)-1-methylethyl]pyridine.

Workup

  1. filtrationThe catalyst is filtered
  2. customthe filtrate evaporated

Sources & evidence

ORD record
ord-fcb16f2057c84a7da51586a21226f5ed
Source dataset
uspto-grants-1981_12
Patent number
USRE030812

Reaction notes

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