HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → Butyl prop-2-enoate;styrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 2-Butoxyethanol | HCID 8133 | — |
| Reactant | Butyl Acrylate | HCID 8846 | — |
| Reactant | 2-Propanimine | HCID 142304 | — |
| Product | Butyl prop-2-enoate;styrene | HCID 168422 | — |
Reaction Steps
The procedure described in part (a) of example 21 is repeated using 1076 g of 2-butoxyethanol, 1780 g of styrene, 730 g of butyl acrylate (BA), an initial charge of 179.2 g of 75% t-BP (in mineral spirits) and a final charge of 17.9 g thereof, a monomer feed time of 4.5 hours and a polymerization temperature of 150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04303563 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-f82bffd5d4a54f0c8e314b5b9b922da4 |
| Source note | uspto-grants-1981_12 |