HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(dibenzylamino)acetate → 2-(N,N-Dibenzylaminomethyl)-4-phenyl-3-chromene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(dibenzylamino)acetate | HCID 3553452 | — |
| Reactant | HCID 178506676 | HCID 178506676 | — |
| Product | 2-(N,N-Dibenzylaminomethyl)-4-phenyl-3-chromene | HCID 86003689 | — |
Reaction Steps
The process of Example 4 was repeated using N,N-dibenzylglycine ethyl ester in place of N,N-dimethylalanine ethyl ester in part (a), then following the precedure in part (b) and in part (c) using phenyl lithium in place of the 4-bromochlorobenzene/butyl lithium, to yield the title compound as an oil, after dehydration in dilute HCl as in part (d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04303656 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-ff1ad44154244157b1e2e1f1471997f7 |
| Source note | uspto-grants-1981_12 |