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HRID1659581

反应详情

EQUATION

反应方程式

HRID 1659581 的结构方程式

REACTANTS

反应物

2
结构：CN(C)Cc1ccc(CSCCN)o1
HCID162203

5-((2-Aminoethyl)thiomethyl)-N,N-dimethyl-2-furanmethanamine

C10H18N2OS

结构：CSC(=NC#N)NCCSCc1ccc(CN(C)C)o1
HCID178503926

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)Cc1ccc(CSCCNC(=NC#N)NCCSCc2ccc(CN(C)C)o2)o1
HCID178483231

未命名化合物

收率 57.1%

PROCEDURE

实验过程

A mixture of 5-[[(2-aminoethyl)thio]methyl]N,N-dimethyl-2-furanmethanamine (1.39 g) and N'-cyano-N-[2-[[5-[(dimethylamino)methyl]-2-furanylmethyl]thio]ethyl]carbamimidothioic acid, methyl ester (2.0 g) was heated at 120° for 2 days. The oily product was subjected to column chromatography (silica-methanol) giving the title compound as a yellow oil (1.75 g).

WORKUP

后处理

  1. temperaturewas heated at 120° for 2 days