HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20559433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | HCID 20559401 | HCID 20559401 | — |
| Product | HCID 20559433 | HCID 20559433 | — |
Reaction Steps
A mixture of 5-[[(2-aminoethyl)thio]methyl]-N-cyclopropyl-2-furanmethanamine (1.67 g) and 1,1-bis-(methylthio)-2-nitroethene (0.61 g) was heated at 98°-100° for 3hr. The oily residue was chromatograpged (silica/methanol-0.88 ammonia 79:1) and the appropriate eluate evaporated to dryness to give the title compound (1.07 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04304780 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-55186b4a895c40f0a593c703e77e8100 |
| Source note | uspto-grants-1981_12 |