HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum ethylate → 3-Phenoxybenzyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum ethylate | HCID 11153 | — |
| Reactant | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Phenoxybenzyl alcohol | HCID 26295 | 98.9% |
Reaction Steps
To a solution of 198 g. of m-phenoxy-benzaldehyde in 1 liter of absolute ethanol 60 g. of aluminum ethoxide are added. The reaction mixture is allowed to stand at room temperature. The reaction mixture is then evaporated under atmospheric pressure. From the residue following the procedure of Example 1 198 g. (98.9%) of m-phenoxybenzyl alcohol are prepared in a purity over 95% (according to gas chromatography).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04304938 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-ac39fed2a49f4867aa4db807882f9c9d |
| Source note | uspto-grants-1981_12 |