HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → Ethyl 4-chloro-3-oxo-2-[(pentyloxy)imino]butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | Ethyl 3-oxo-2-[(pentyloxy)imino]butanoate | HCID 53697317 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Ethyl 4-chloro-3-oxo-2-[(pentyloxy)imino]butanoate | HCID 53992771 | — |
Reaction Steps
Ethyl 2-pentyloxyimino-3-oxobutyrate (syn isomer) (57.5 g.) and sulfuryl chloride (20.9 ml.) were reacted in acetic acid (58.5 ml.) according to a similar manner to that of Preparation (6-10) to give an oil of ethyl 2-pentyloxyimino-3-oxo-4-chlorobutyrate (syn isomer) (51.1 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04304770 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-be197f407bb147f4a04c83451c06f566 |
| Source note | uspto-grants-1981_12 |