HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 54050120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 4-Fluorobenzyl chloride | HCID 9602 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54050120 | HCID 54050120 | 95.9% |
Reaction Steps
Ethyl2-hydroxyimino-3-oxobutyrate (syn isomer, 40.0 g.), 4-fluorobenzyl chloride (43.6 g.), N,N-dimethylformamide (60.0 ml), potassium carbonate (52.0 g.) and ethyl acetate (60.0 ml.) were treated in a conventional manner to give ethyl 2-(4-fluorobenzyloxyimino)-3-oxobutyrate (syn isomer, 64.4 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04304770 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-c7bb356b629c47989052c8268be4bd22 |
| Source note | uspto-grants-1981_12 |