Water → HCID 20558416, compound

Participants

Reaction Conditions

Reaction Steps

Into 120 ml of water, one adds 28 g of iron powder and 10 ml of acetic acid. The mixture is brought to a temperature of 85° C. under agitation. Then one adds, little by little, 0.1 mol (28 g) of 2-diethylcarbamylmethylamino-4-nitro anisole. The reaction medium is maintained for 10 minutes at a temperature of 90° C. Then one adds 14 ml of 10 N. soda solution. It is filtered boiling on a heated filter. By cooling the filtrate the expected product crystallizes. After recrystallization in water and vacuum drying it melts at 111° C.

Provenance & Evidence