HRID1659909

反应详情

EQUATION

反应方程式

HRID 1659909 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

40.2 g of 2,3-dimethylbenzothiazolium tosylate and 7.32 g of salicylic aldehyde were mixed in 1200 ml of ethanol; to this mixture were added 12 ml of piperidine with stirring. Stirring was continued for 1 hour at room temperature. A precipitate was formed which was filtered out and washed with ethanol.

WORKUP

后处理

  1. stirringStirring
  2. customA precipitate was formed which
  3. filtrationwas filtered out
  4. washwashed with ethanol