HRID1659909
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
40.2 g of 2,3-dimethylbenzothiazolium tosylate and 7.32 g of salicylic aldehyde were mixed in 1200 ml of ethanol; to this mixture were added 12 ml of piperidine with stirring. Stirring was continued for 1 hour at room temperature. A precipitate was formed which was filtered out and washed with ethanol.
WORKUP
后处理
- stirringStirring
- customA precipitate was formed which
- filtrationwas filtered out
- washwashed with ethanol