HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Alanine → HCID 178476535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Alanine | HCID 5950 | — |
| Reactant | L-Aspartic Acid | HCID 5960 | — |
| Reactant | L-Lysine | HCID 5962 | — |
| Reactant | L-Valine | HCID 6287 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 178418600 | HCID 178418600 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Solvent | HCID 18475367 | HCID 18475367 | — |
| Product | HCID 178476535 | HCID 178476535 | — |
Reaction Steps
Amino acid analysis following methane sulfonic acid hydrolysis gives the following ratios: Ala 1.00; Val 1.07; Lys 1.02; Arg 1.02; Asp 1.06. TLC data: Rf =0.17 in 4:1:1:2 (n-butanol-acetic acid-pyridine-water) on silica plates. Rf =0.40 in 4:1:1:2 on cellulose plates. Analysis of the product by high pressure liquid chromatography on a μ Bondapak C18 column (97% 0.1 M ammonium acetate: 3% acetonitrile, pH 4.0) shows the product to be 98% pure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04305852 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-dfba79a1930c4a3bb7bfefaeb3264536 |
| Source note | uspto-grants-1981_12 |