反应详情

A mixture of 400 mg. (0.988 mmole) of 3-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]cyclohex-2-enone and 20 mg. of 5% palladium-on-carbon was stirred under one atmosphere of hydrogen pressure for 30 minutes. The reaction mixture was then filtered through diatomaceous earth with ether and the filtrate evaporated to a solid. The crude solid was recrystallized from petroleum ether to yield 110 mg. (35%) of the title compound, M.P. 122°-123° C.

1. additionA mixture of 400 mg
2. filtrationThe reaction mixture was then filtered through diatomaceous earth with ether
3. customthe filtrate evaporated to a solid
4. customThe crude solid was recrystallized from petroleum ether
5. customto yield 110 mg